Redefining Sample Pump Flow Measurement



(https://www.skcinc.com/catalog/pdf/instructions/1919.pdf)

History

The industrial hygiene profession has traditionally described pump calibrators as primary standards if the flow measurements involved the direct measurement of volume on the basis of the physical dimensions of a defined closed space. An example of a primary standard according to this definition is the soap bubble meter (film flowmeter). Historically, secondary standards have been described as instruments that trace their calibration to primary standards and maintain their accuracy with reasonable care and handling. Examples of secondary standards include rotameters and wet test meters.

Redefining Calibrators

In industrial hygiene, the terms “primary” and “secondary” have become accepted as general descriptions for various calibration devices, but they are not officially adopted industry standards. Even U.S. OSHA states in its Technical Manual (Appendix F) that it no longer considers inverted burets to be primary calibration standards. In addition, these historical descriptions should not be confused with precise definitions from the National Institute of Standards and Technology (NIST), the U.S. national standards laboratory and metrological traceability organization responsible for maintaining the physical standards upon which measurements in the U.S. are based. Following are what we find to be the clearest definitions of primary and secondary standards:

A primary standard in metrology is sufficiently accurate such that it is not calibrated by or subordinate to other standards. Primary standards are defined by quantities such as length, mass, and time. Their value is accepted without reference to other standards of the same quantity. Standards used in industrial hygiene for calibrating sample pumps do not meet this strict definition of a primary standard.

Secondary standards are calibrated with reference to a primary standard and are very close approximations of primary reference standards. Calibration standards used in industrial hygiene meet this definition.

Where does the SKC chek-mate Calibrator fit?

Using the definitions above, the SKC chek-mate Calibrator is technically a secondary standard; however, in the ACGIH publication Air Sampling Instruments, 9th Edition (page 151), a highly accurate secondary standard calibrator is defined as follows: “Among secondary standards, however, there are a number of instruments that provide an accuracy nearly comparable to that of primary standards but which, of themselves, cannot be calibrated by internal volume measurement. These instruments are sometimes referred to as intermediate standards and provide an accuracy of approximately 1.0 %.” The SKC chek-mate Calibrator meets this definition with a volumetric accuracy of 1% of reading and high repeatability; therefore, SKC identifies the chek-mate as an intermediate standard. Each chek-mate is calibrated in a calibration laboratory with accuracy certified by NIST and backed by ISO 17025 accreditation. A NIST-traceable calibration certificate is shipped with each chek-mate. UKAS calibration and certificates are available for customers in the U.K. and other countries.

Summary

In the absence of industry standards for calibrator designations, health and safety professionals should base selection of a pump calibrator on its usability, stated accuracy, repeatability, and certificate of verification to a higher standard such as NIST and not on the principle of operation or designation. The SKC chek-mate Calibrator is very easy to use in the lab or field, provides accuracy nearly comparable to that of primary standards, and is NIST traceable. If a standard designation is required, the SKC chek-mate falls squarely in the intermediate standard category.

Here is the example of the submission letter containing the basic elements required by a scientific journal. (Note: Apart from the common statements a scientific journal may require some additional information that should be included in your submission letter. So, always make sure that your submission letter contains all required statements described in your target journal's author guidelines).

 

Edward Marriot University of Research 72 Green Street LONDON EC8Y 5SY GREAT BRITAIN   Prof. Donald Richards Editor-in-Chief Journal of Engineering for the Marine Environment Puyit Publications Ltd 1 Oliver's Yard 55 City Road MONTREAL QC P8W CANADA Phone: +1 (0) 20 7 924 8500 ; Fax: +1 (0) 20 7 924 8600 E-mail: market@puyit.ca.   October 13, 2017   Dear Prof. Richards,   We are pleased to submit an original research article entitled “Mathematical Model of Oil-Containing Water Purification Process in the Volume of Granulated Media” for consideration for publication in Journal of Engineering for the Marine Environment. In our research paper we developed the mathematical model of oil-containing water purification process in the volume of granulated media. On the basis of this model we studied purifying ability of filtering unit with granulated coalescing media, which regenerates filtering media in the mode of pseudo liquefaction of granule without disassembling and replacement of filtering element. We confirm that this model allows to calculate the rational constructive and operational parameters of the plant with granulated filter elements. We believe that the manuscript is appropriate for publication by Journal of Engineering for the Marine Environment since it focuses on advances in new techniques that enable better understanding and utilization of the life cycle of maritime assets in the maritime environment as well as the increase of their efficiency). The manuscript is original. No part of the manuscript has been published before, nor is any part of it under consideration for publication at another journal. There are no conflicts of interest to disclose.   Thank you for your consideration.   Sincerely,   Edward Marriot, PhD Professor, Department of Marine Environment University of Research Phone: +44 (0)11 2 1177 E-mail : E.Marriot@edu.co.uk

 

            Draft the article submission letter in compliance with the requirements of a scientific journal. Visit 'Manuscript Submission Guidelines' or 'Instructions for Authors' of the target journal (the list of probable scientific journals: ~Advances in Physics; ~Annual Review of Biophysics; ~ Advanced Functional Materials; ~ Materials Today; ~ International Journal of Computer Vision; ~ Foundation and Trends in Machine Learning; ~ IEEE Wireless Communication; ~ Foundation and Trends in Computer Graphics)


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